The CIA method is much more work: you first mill the charcoal and sulfur together (just like you would with the ball mill method), but this is followed by dissolving the potassium nitrate in hot boiling water which is then mixed with the milled charcoal/sulfur mixture.
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Aryl chlorides and bromides are formed from arenes in a ball mill using KHSO5 and NaX (X = Cl, Br) as oxidant and halogen source, respectively. Investigation of the reaction parameters identified operating frequency, milling time, and the number of milling balls as the main influencing variables, as these de
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Opening the ball mill box reveals a user's manual, a mill base, two mill jars, and five extra drive belts. Unpacking the Ball Mill The ball mill jars The first thing that struck me when I first looked at these mills was the nice quality of the mill jars. These things are really heavyduty, and have a very solid closing and sealinglid assembly.
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